Synthesis of Single Crystal ZSM-5 by Solid-like State Conversion

S. Chen; S. Y. Han; Y. Liu; D. D. Guan; N. Z. Jiang; W. Meng

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Paper

Synthesis of Single Crystal ZSM-5 by Solid-like State Conversion

In Proceedings of the International Workshop on Materials, Chemistry and Engineering IWMCE - Volume 1, 330-335, 2018 , Xiamen, China

Authors: S. Chen ; S. Y. Han ; Y. Liu ; D. D. Guan ; N. Z. Jiang and W. Meng

Affiliation: Department of Chemistry, College of Science and Yanbian University, China

Keyword(s): ZSM-5; single crystal; solid-like state conversion

Abstract: ZSM-5 single crystals were synthesized from fumed silica via solid-like state conversion. The properties of synthesized zeolite samples were characterized by XRD, SEM, 27Al MAS NMR spectra, XRF and NH3-TPD. The results showed that the amorphous solid phase could be converted into ZSM-5 zeolites with cubic-like crystal morphology at temperature range of 160oC-190oC within 24 h. The optimum synthesis condition is at 180oC for 16 h by considering the crystallinity and uniformity of zeolites. The conversion of toluene in gas phase disproportionation over optimized ZSM-5 catalyst raised to 40.18%, which is higher than commercial ZSM-5 zeolite.

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Paper citation in several formats:

Chen, S.; Han, S.; Liu, Y.; Guan, D.; Jiang, N. and Meng, W. (2018). Synthesis of Single Crystal ZSM-5 by Solid-like State Conversion. In Proceedings of the International Workshop on Materials, Chemistry and Engineering - IWMCE; ISBN 978-989-758-346-9, SciTePress, pages 330-335. DOI: 10.5220/0007438403300335

@conference{iwmce18,
author={S. Chen. and S. Y. Han. and Y. Liu. and D. D. Guan. and N. Z. Jiang. and W. Meng.},
title={Synthesis of Single Crystal ZSM-5 by Solid-like State Conversion},
booktitle={Proceedings of the International Workshop on Materials, Chemistry and Engineering - IWMCE},
year={2018},
pages={330-335},
publisher={SciTePress},
organization={INSTICC},
doi={10.5220/0007438403300335},
isbn={978-989-758-346-9},
}

TY - CONF

JO - Proceedings of the International Workshop on Materials, Chemistry and Engineering - IWMCE
TI - Synthesis of Single Crystal ZSM-5 by Solid-like State Conversion
SN - 978-989-758-346-9
AU - Chen, S.
AU - Han, S.
AU - Liu, Y.
AU - Guan, D.
AU - Jiang, N.
AU - Meng, W.
PY - 2018
SP - 330
EP - 335
DO - 10.5220/0007438403300335
PB - SciTePress